Beamline I311, MAX-lab, Lund, Sweden

From undulator to end station

By changing the gap value of the undulator, the energy position of the undulator peaks can be varied over a wide energy range. This enables maximizing the photon intensity output at any energy. The new undulator magnets (since summer 2010) provide us with light from 42.5 eV and upwards (period = 54.4 mm, 45 periods, K_eff = 4.31).The characteristics of the undulator are summarized in the two following tables (using a 1220 lines/mm monochromator):

At Kmax (small gap values) and making use of the large horizontal acceptance angle of the beamline (3 mrad) the undulator behaves more like a multipole wiggler above about 600 eV photon energy, i.e. it will give a smooth spectrum with only weak undulator features. At larger gaps the undulator also has a so-called tapering possibility, i.e. the distance between the upper and lower magnet assemblies can be set different for the front and the rear end of the undulator thereby allowing detuning from "perfect" undulator enhancement. This can turn out to be of great value when recording absorption spectra as the peak intensity gets stretched over a larger photon energy range.

Beamline layout

The light from the undulator is focussed horizontally by means of a cylindrical pre-mirror (M1). The plane mirror (M2) moves synchronously with the monochromator grating (G), and is followed by a spherical mirror (M3). This arrangement keeps the image of the virtual source (S') fixed on the exit slit (S1) position for each value of the fixed focus constant Cff.

The re-focusing system consists of two spherical mirrors mounted in a Kirkpatrick–Baez arrangement. The vertically deflecting mirror (M4) focuses the exit slit onto the sample while the horizontally deflecting mirror (M5) images the focus of M1 onto the sample position. With a fixed radius of M4 the vertical focusing is optimal only for a specific exit slit position which was chosen to correspond to a Cff value of 4.5. The spot size on the sample is then about 0.5 mm horizontally and 0.1 mm vertically.



The original design of the beamline is described in detail in the following article:

R. Nyholm, J.N. Andersen, U. Johansson, B.N. Jensen and I. Lindau, Beamline I311 at MAX-lab: A VUV/Soft X-Ray Undulator Beamline for High Resolution Electron Spectroscopy, Nucl. Instr. and Meth. in Phys. Res. A 467-468, 520 (2001).
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Monochromator

The modified plane grating Zeiss SX-700 monochromator houses 3 gratings - first, there is the new 1220 lines/mm grating, which was installed in Dec 2007. The old 1220 lines/mm grating is also still there, and has been thoroughly cleaned. As a result, the intensity on the beamline towards higher photon energies has increased significantly, providing a factor of 10 more photon intensity around 1000 eV than before the re-shuffle and cleaning. Both of these gratings can be used for the spectroscopy station (with the new 1220 being the default).

The 1220 lines/mm monochromators can be operated at different Cff values, with a corresponding position of the moveable exit slit. Increasing the C value gives better resolution with worse 2nd order suppression, whilst lowering the C value does the opposite. C = 2.25 is the most commonly used and gives the best compromise of flux, resolution and 2nd order rejection.

The third grating has 300 lines/mm, and provides the intense light needed for the PEEM station.


Exit slit, photodiode and mesh

A GaAsP photodiode is installed just after the exit slit, which can be used to estimate the photon flux or get a background spectrum for NEXAFS measurements. For the same purpose, a gold mesh is installed in the last beamline compartment before the spectroscopy end station. When they are put into the beam, the photodiode blocks the light completely, whilst the Au-mesh takes away 50% of the light. Below are the tables for the exit slit settings, as well as the diode sensitivity:

Photon Resolution tests

The ultimate performance of the 1220 lines/mm monochromator grating has been tested using X-ray absorption spectroscopy on gases. Examples can be found here. The curve below illustrates the energy resolution of the 1220 lines/mm monochromators over the entire photon energy region.




Beamline I311

Contact

I311 (Spectroscopy):
Karina Schulte

E-mail:
karina.schulte (at) maxlab.lu.se

Phone (Office):
+46 46 222 4331

Mobile:
+46 709 323 020



I311 (PEEM):
Alexei Zakharov

E-mail:
alexei.zakharov (at) maxlab.lu.se

Phone (Office):
+46 46 222 3357

Mobile:
+46 733 439 556



I311 (Overall):
Jesper Andersen

E-mail:
jesper.andersen (at) sljus.lu.se

Phone (Office):
+46 46 222 4153



Address for deliveries

Beamline I311
MAX-lab
Lund Universitet
Ole Römersväg 1
223 63 Lund, SWEDEN



Phone (I311 Hutch):
+46 46 222 0115
Fax (MAX-lab):
+46 46 222 4710

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