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Last modified: 2010-10-18

Beamline I911-1 - Short information

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Beamline I911-1 is presently equipped with set-up for nano-science and x-ray physics education. It is one out of five experiment stations at beamline I911. The experiment hutch includs a set-up for fluorescence measurements to determine x-ray scattering factors and to scan an absorption edge (x-ray physics education) and a set-up for studying mono-layers on a water substrate with grazing incidence measurements using the synchrotron radiation and reflectivity measurements using an additional x-ray source.

I911-1 is planned to eventually be equipped as a fixed wavelength station for macromolecular crystallography. The wavelength, 1.2 Å, for the future macromolecular crystalllography station is chosen to have a high flux and somewhat longer wavelength than the other fixed wavelength stations at I911. The beam is first monochromatized and horizontally focused by a planar diamond crystal working in Laue geometry and then focused in the vertical by a 400 mm, curved multi-layer mirror. The high-flux photon beam is produced by a super-conducting multi-pole wiggler.

Contact persons (see also the beamline homepage):

Thomas Ursby, Beamline Manager I911

Robert Feidenhans'l, responsible for present set-up

References:

C.B. Mammen, T. Ursby, M. Thunnissen and J. Als-Nielsen, Bent Diamond Crystals and Multilayer Based Optics at the new 5-Station Protein Crystallography Beamline `Cassiopeia' at MAX-lab, AIP Conference Proceedings, 705, 808-811, 2004.

C.B. Mammen, T Ursby, Y Cerenius, M Thunnissen, J Als-Nielsen, S Larsen and A. Liljas, Design of a 5-Station Macromolecular Crystallography Beamline at MAX-lab, Acta Physica Polonica A, 101, 595, 2002.

Technical data:

Source

Multi-pole wiggler, period= 61 mm, 49 poles, Bmax = 3.5 T.

Monochromator 

Diamond crystal, horizontally focusing.

Mirror 

Multilayer mirror, curved to focus in the vertical (R = 400 m). 

Wavelength

1.2 Å with some tunability

Wavelength resolution

 E/dE ~ 103

Photon flux on sample 

3 x 1011 photons / s in full beam (measured)

Spot size on sample

0.4(h) x 0.2(v) mm2 (calculated)

Experimental techniques 

Grazing incidence and x-ray reflectivity measurements

Fluorescence measurements

(Later macromolecular crystallography)