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Beamline I911-1 is presently equipped with set-up for nano-science and x-ray physics education. It is one out of five experiment stations at beamline I911. The experiment hutch includs a set-up for fluorescence measurements to determine x-ray scattering factors and to scan an absorption edge (x-ray physics education) and a set-up for studying mono-layers on a water substrate with grazing incidence measurements using the synchrotron radiation and reflectivity measurements using an additional x-ray source.
I911-1 is planned to eventually be equipped as a fixed wavelength station for macromolecular crystallography. The wavelength, 1.25 Å, for the future macromolecular crystalllography station is chosen to have a high flux and somewhat longer wavelength than the other fixed wavelength stations at I911. The beam is first monochromatized and horizontally focused by a planar diamond crystal working in Laue geometry and then focused in the vertical by a 400 mm, curved multi-layer mirror. The high-flux photon beam is produced by a super-conducting multi-pole wiggler.
Thomas Ursby, Beamline Manager I911
Robert Feidenhans'l, responsible for present set-up
References:
C.B. Mammen, T. Ursby, M. Thunnissen and J. Als-Nielsen, Bent Diamond Crystals and Multilayer Based Optics at the new 5-Station Protein Crystallography Beamline `Cassiopeia' at MAX-lab, AIP Conference Proceedings, 705, 808-811, 2004.
C.B. Mammen, T Ursby, Y Cerenius, M Thunnissen, J Als-Nielsen, S Larsen and A. Liljas, Design of a 5-Station Macromolecular Crystallography Beamline at MAX-lab, Acta Physica Polonica A, 101, 595, 2002.
Technical data:
| Source |
Multi-pole wiggler, period= 61 mm, 49 poles, Bmax = 3.5 T. |
| Monochromator |
Diamond crystal, horizontally focusing. |
| Mirror |
Multilayer mirror, curved to focus in the vertical (R = 400 m). |
| Wavelength |
1.04 Å with some tunability (later planned to be 1.25 Å) |
| Wavelength resolution |
E/dE ~ 103 |
| Photon flux on sample |
3 x 1011 photons / s in full beam (measured) |
| Spot size on sample |
0.4(h) x 0.2(v) mm2 (calculated) |
| Experimental techniques |
Grazing incidence and x-ray reflectivity measurements
Fluorescence measurements
(Later macromolecular crystallography)
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